Sensitive determination of mercury by magnetic dispersive solid-phase extraction combined with flow-injection-cold vapour-graphite furnace atomic absorption spectrometry

Highly sensitive determination of cadmium and lead in leached solutions from ceramic ware by graphite furnace atomic absorption spectrometry coupled with sequential injection-based solid phase extraction method.

A fully automated pretreatment system based on sequential injection solid-phase extraction (SPE) coupled to a graphite furnace atomic absorption spectrometer (Auto-Pret-GFAAS system) was developed to determine trace amounts of cadmium and lead. A handmade minicolumn packed with a chelating resin was used for the preconcentration of both metals. All protocol for the on-line SPE method was contro...

GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY WITH MAlIlRIX MODIFICATION FOR DETERMINATION OF LEAD IN DRINKING WATER

An amoniumvanadate plus sodium molybdate mixed modifier Graphite Furnace Atomic Absorption Spectrometric method has been developed for determination of traces of lead in drinking water. The concentration of lead in the sample is obtained by direct comparison to linear working graph prepared from aqueous standards in the modifier medium, The results indicate the better performance of the pro...

Determination of total mercury in biological tissues by flow injection cold vapour generation atomic absorption spectrometry following tetramethylammonium hydroxide digestion.

A simple, rapid and reliable method was developed for the determination of total mercury in biological samples. Samples were solubilized using tetramethylammonium hydroxide (TMAH). The organically bound mercury was cleaved and converted to inorganic mercury by on-line addition of KMnO4. The decomposed mercury together with inorganic mercury originally present in samples was determined by flow i...

Determination of total mercury in bauxite and bauxite residue by flow injection cold vapour atomic absorption spectrometry

Preconcentration and determination of palladium water samples by ionic liquid - dispersive liquid liquid microextraction combined with flame atomic absorption spectrometry

A simple, rapid and efficient dispersive liquid–liquid microextraction by use of ionic liquid (IL-DLLME)method, followed by flame atomic absorption spectrometry (FAAS) was developed for the preconcentrationand determination of palladium in water samples. In this method, an appropriate mixture of acetone and octylmethyl imidazolium hexafluorophosphate was injected rapidly into the aqueous sample...